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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1707224Generated: November 1, 2026

Cyclohexyl isocyanate → HCID 23192921, compound

https://huagongshe.com/reaction/1707224

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyclohexyl isocyanateHCID 18502—
Reactant1-(1-Isocyanato-1-methylethyl)-3-(1-methylethenyl)benzeneHCID 604152—
ProductHCID 23192921HCID 23192921—

Reaction Conditions

Temperature150 °C

Reaction Steps

We combined 0.0830 g TPAO, 60.41 g of m-TMI, and 25.04 g cyclohexylisocyanate. After heating at 150° C. for 7 hours, IR showed nearly complete conversion of isocyanates to carbodiimides. 1H--NMR indicated the desired product contaminated with 1,3-dicyclohexylcarbodiimide, and 1,3-bis[2-(3-isopropenylphenyl)-2propyl]carbodiimide.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05352400
Source datasetuspto-grants-1994_10
ORD IDord-efb174a63a68432a8b04e01ff822c804
Source noteuspto-grants-1994_10