HRID1707233

反应详情

EQUATION

反应方程式

HRID 1707233 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

First, 0.5 g of platinum oxide was added to a solution formed by dissolving 25.3 g of 1-methyl-1-[3-(1-methylethenyl)phenyl]ethylamine in 100 ml of ethyl alcohol, and a hydrogenation reaction was then carried out at a temperature of 15° to 35° C. for 7 hours under atmospheric pressure under a hydrogen gas stream. Afterward, reaction residues were removed by filtration, and the resultant filtrate was then concentrated to obtain 25.0 g of 1-methyl-1-[3-(1-methylethyl)phenyl]ethylamine.

WORKUP

后处理

  1. customformed
  2. customa hydrogenation reaction
  3. customAfterward, reaction residues
  4. customwere removed by filtration
  5. concentrationthe resultant filtrate was then concentrated