HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-(Benzo[d][1,3]dioxol-5-yl)-1,4-dioxaspiro[4.5]decan-8-ol → 1,4-Dioxaspiro[4.5]dec-7-ene, 8-(1,3-benzodioxol-5-yl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-(Benzo[d][1,3]dioxol-5-yl)-1,4-dioxaspiro[4.5]decan-8-ol | HCID 10912840 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1,4-Dioxaspiro[4.5]dec-7-ene, 8-(1,3-benzodioxol-5-yl)- | HCID 13855633 | 73% |
Reaction Steps
A solution of 8-(1,3-benzodioxol-5-yl)-1,4-dioxaspiro[4.5]decan-8-ol in toluene was reacted as described in example 2 to give the product (73%, mp: 75°-76° C). Calc'd for C15H16O4 : C, 69.22%; H, 6.20%. Found: C, 69.19%; H, 6.14%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05352678 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-ab7823056dc041c6b822542092b77e54 |
| Source note | uspto-grants-1994_10 |