HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminocyclohex-2-en-1-one → HCID 67819953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminocyclohex-2-en-1-one | HCID 78892 | — |
| Reactant | HCID 54466936 | HCID 54466936 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67819953 | HCID 67819953 | — |
Reaction Steps
37 g (0.33 mol) 3-aminocyclohex-2-en-1-one and 42 g (0.13 mol) 1-chloro-7-(3-nitrophenyl-methylene)-nonane-6,8-dione are boiled under reflux in 400 ml methanol for 38 h. The mixture is concentrated and the residue is chromatographed with toluene/acetone=8/2. The title compound is obtained as a yellow oil. Yield: 18 g (34%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05352684 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-0b5daf2af619455ab49e5acc56c9f943 |
| Source note | uspto-grants-1994_10 |