Methyl iodide → HCID 18963043, compound

HRID 1707302Notes

Reaction equation

[CH2:1]([O:8][C:9]1[C:14]([OH:15])=[CH:13][C:12]([CH2:16][CH3:17])=[CH:11][C:10]=1[O:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][C:24]([C:27]#[N:28])([CH3:26])[CH3:25])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:29]I>>[CH2:1]([O:8][C:9]1[C:14]([O:15][CH3:29])=[CH:13][C:12]([CH2:16][CH3:17])=[CH:11][C:10]=1[O:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][C:24]([C:27]#[N:28])([CH3:25])[CH3:26])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 18963052HCID 18963052, compound

Product 1

HCID 18963043HCID 18963043, compoundYield 75%

Procedure

1-Benzyloxy-2-(6-cyano-6-methylheptyloxy)-4-ethyl -6-methoxy benzene was prepared in 75% yield as a white solid from 1-Benzyloxy-2-(6-cyano-6-methylheptyloxy)-4-ethyl-6-hydroxy benzene and methyliodide.

Sources & evidence

ORD record: ord-0b8e74ab849c43f98f2de110963a71d7
Source dataset: uspto-grants-1994_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05352690

Reaction notes

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