Isopropyl iodide → HCID 18963021, compound

HRID 1707305Notes

Reaction equation

[CH2:1]([O:8][C:9]1[C:14]([OH:15])=[CH:13][C:12]([CH2:16][CH3:17])=[C:11]([O:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][C:24]([C:27]#[N:28])([CH3:26])[CH3:25])[CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.I[CH:30]([CH3:32])[CH3:31]>>[CH2:1]([O:8][C:9]1[C:14]([O:15][CH:30]([CH3:32])[CH3:31])=[CH:13][C:12]([CH2:16][CH3:17])=[C:11]([O:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][C:24]([C:27]#[N:28])([CH3:25])[CH3:26])[CH:10]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

Reactant 2

HCID 6362Isopropyl iodide

HCID 18963022HCID 18963022, compound

Product 1

HCID 18963021HCID 18963021, compoundYield 100%

Procedure

1-Benzyloxy-3-(6-cyano-6-methylheptyloxy)-4-ethyl -6-isopropoxy benzene was prepared in 100% yield as a white solid from 1-Benzyloxy-3-(6-cyano-6-methylheptyloxy)-4-ethyl-6-hydroxy benzene and 2-iodo-propane.

Sources & evidence

ORD record: ord-f28cfa22343a4a88a4f05d45c0a4a691
Source dataset: uspto-grants-1994_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05352690

Reaction notes

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