Bromocyclopentane → HCID 18963055, compound

HRID 1707306Notes

Reaction equation

HRID 1707306 reaction equation
[CH2:1]([O:8][C:9]1[C:14]([OH:15])=[CH:13][C:12]([CH2:16][CH3:17])=[CH:11][C:10]=1[O:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][C:24]([C:27]#[N:28])([CH3:26])[CH3:25])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Br[CH:30]1[CH2:34][CH2:33][CH2:32][CH2:31]1>>[CH2:1]([O:8][C:9]1[C:14]([O:15][CH:30]2[CH2:34][CH2:33][CH2:32][CH2:31]2)=[CH:13][C:12]([CH2:16][CH3:17])=[CH:11][C:10]=1[O:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][C:24]([C:27]#[N:28])([CH3:25])[CH3:26])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 8728BromocyclopentaneHCID 18963052HCID 18963052, compound

Product 1

HCID 18963055HCID 18963055, compoundYield 92%

Procedure

1-Benzyloxy-2-(6-cyano-6-methylheptyloxy)-4-ethyl-6-cyclopentyloxy benzene was prepared in 92% yield as a white solid from 1-Benzyloxy-2-(6-cyano-6-methylheptyloxy)-4-ethyl-6-hydroxy benzene and bromo-cyclopentane.

Sources & evidence

ORD record
ord-d2a81cf5cbe941799d1d26187dc7919a
Source dataset
uspto-grants-1994_10
Patent number
US05352690

Reaction notes

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