1-Bromo-3-methylbutane → 1-(3-Methylbutyl)-3-propionyl pyridinium bromide

HRID 1707344Notes

Reaction equation

HRID 1707344 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7]([CH2:9][CH3:10])=[O:8])[CH:2]=1.[Br:11][CH2:12][CH2:13][CH:14]([CH3:16])[CH3:15]>>[Br-:11].[CH3:15][CH:14]([CH3:16])[CH2:13][CH2:12][N+:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7](=[O:8])[CH2:9][CH3:10])[CH:2]=1

Participants

3

Reactant 2

HCID 78911-Bromo-3-methylbutaneHCID 740741-(3-Pyridyl)propan-1-one

Product 1

HCID 189633821-(3-Methylbutyl)-3-propionyl pyridinium bromide

Procedure

Ethyl 3-pyridyl ketone was reacted with 1-bromo-3-methylbutane according to the procedure of Parb a) of Example 6 to give 1-(3-methylbutyl)-3-propionyl pyridinium bromide as a pale brown crystalline solid.

Sources & evidence

ORD record
ord-247771f95c1b42ef950b5d0427a08a42
Source dataset
uspto-grants-1994_10
Patent number
US05352793

Reaction notes

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