1-Chloro-3-methyl-2-butene → 1-(3-Methyl-2-butenyl)-3-butyryl pyridinium chloride

HRID 1707347Notes

Reaction equation

HRID 1707347 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7]([CH2:9][CH2:10][CH3:11])=[O:8])[CH:2]=1.[Cl:12][CH2:13][CH:14]=[C:15]([CH3:17])[CH3:16]>>[Cl-:12].[CH3:16][C:15]([CH3:17])=[CH:14][CH2:13][N+:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7](=[O:8])[CH2:9][CH2:10][CH3:11])[CH:2]=1

Participants

3

Reactant 2

HCID 104291-Chloro-3-methyl-2-buteneHCID 4595021-(Pyridin-3-yl)butan-1-one

Product 1

HCID 189633791-(3-Methyl-2-butenyl)-3-butyryl pyridinium chloride

Procedure

Propyl 3-pyridyl ketone was reacted with 1-chloro-3-methyl-2-butene according to the procedure of Part a) of Example 4 to give 1-(3-methyl-2-butenyl)-3-butyryl pyridinium chloride as a cream coloured crystalline solid.

Sources & evidence

ORD record
ord-0970c4ce00ec41408c017409128a02c3
Source dataset
uspto-grants-1994_10
Patent number
US05352793

Reaction notes

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