m-Anisoyl chloride → HCID 18963378, compound

HRID 1707352Notes

Reaction equation

HRID 1707352 reaction equation
[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[NH:9][CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1.[CH3:14][O:15][C:16]1[CH:17]=[C:18]([CH:22]=[CH:23][CH:24]=1)[C:19](Cl)=[O:20]>>[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[N:9]([C:19](=[O:20])[C:18]3[CH:22]=[CH:23][CH:24]=[C:16]([O:15][CH3:14])[CH:17]=3)[CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1

Participants

3

Reactant 2

HCID 74374m-Anisoyl chlorideHCID 118196217,7-Dimethyl-2,3,4,6,7,8-hexahydroquinolin-5(1H)-one

Product 1

HCID 18963378HCID 18963378, compound

Procedure

7,7-Dimethyl-1,2,3,4,7,8-hexahydro-quinolin-5(6H)-one was reacted with 3-methoxybenzoyl chloride according to the procedure of Part b) of Example 1 to give 7,7-dimethyl-1,2,3,4,7,8-hexahydro-1-(3-methoxybenzoyl)-quinolin-5(6H)-one (20) as a pale yellow solid.

Sources & evidence

ORD record
ord-087b035da4a3477b98c90d3eabff0c51
Source dataset
uspto-grants-1994_10
Patent number
US05352793

Reaction notes

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