HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetic Acid → 2-(2,5-Dichlorophenyl)-2-mercaptoacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetic Acid | HCID 300 | — |
| Reactant | 2,5-Dichloroaniline | HCID 7262 | — |
| Reactant | 2,5-Dichlorobenzenethiol | HCID 79965 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Catalyst | Copper Sulfate | HCID 24462 | — |
| Product | 2-(2,5-Dichlorophenyl)-2-mercaptoacetic acid | HCID 22492329 | — |
Reaction Steps
the method in which 2,5-dichloroaniline is diazotized and then reacted with thiourea in the presence of copper sulfate and subsequently hydrolyzed to 2,5-dichlorothiophenol, followed by reaction with monochloroacetic acid to yield 2,5-dichlorophenylthioglycolic acid (Ger. Offen. DE3715508),
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05352821 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-0bbcd9b1adf24fcb9865ee5977c1ea2d |
| Source note | uspto-grants-1994_10 |