Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Dodecanol | HCID 8193 | — |
| Reactant | Dibutyltin oxide | HCID 61221 | — |
| Reactant | HCID 18974158 | HCID 18974158 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18961456 | HCID 18961456 | — |
Reaction Steps
30.6 g (0.1 mol) of methyl-2-methyl-3-(3',5'-di-tert.-butyl-4'-hydroxyphenyl)-propionate and 18.6 g (0.1 mol) of 1-dodecanol are placed in a 4-necked glass flask and heated to 100° C., then 0.25 g=1 mol % of dibutyltin oxide is added and the mixture is heated further to 180° C., with methanol being split off. The reaction mixture is maintained at 180° C. for 6 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05354486 |
|---|
| Source dataset | uspto-grants-1994_10 |
|---|
| ORD ID | ord-685e79c3296d4b99b210522c8f735f5a |
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| Source note | uspto-grants-1994_10 |
|---|
