Benzene → HCID 14817906, compound

Participants

Reaction Steps

A solution of methacryloyl isocyanate (11.1 g; 100 mmol) in dichloroethane (22 g) and methyl p-hydroxybenzoic acid (15.0 g; 100 mmol) were added to benzene (30 g), and the resultant mixture was heated at 80° C. under reflux for 60 minutes. The solvent was removed by evaporation under reduced pressure to give p-methoxycarbonylphenyl N-methacryloylcarbamate as crude crystals. Recrystallization from a mixture of hexane and chloroform gave colorless prisms. M.P., 98°-100° C.

Provenance & Evidence