HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Decylpiperazine → 8-Chloro-10-[(4-decyl-1-piperazinyl)carbonyl]-10,11-dihydrodibenz[b,f][1,4]oxazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Decylpiperazine | HCID 230544 | — |
| Reactant | 8-chlorodibenz[b,f][1,4]oxazepin-10(11H)carbonyl chloride | HCID 14975983 | — |
| Product | 8-Chloro-10-[(4-decyl-1-piperazinyl)carbonyl]-10,11-dihydrodibenz[b,f][1,4]oxazepine | HCID 15224907 | 65.6% |
Reaction Steps
The title compound of Example 2 (1.0 g, 3.4 mmol) was combined with 1-decylpiperazine (0.77 g, 3.4 mmol) and the reaction was carried out by the method of Example 4. Following chromatographic purification, 1.08 g of the title product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05354747 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-7292117e66944ab7bcea97f3274794c0 |
| Source note | uspto-grants-1994_10 |