HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Isopropylpiperazine → HCID 15224910, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Isopropylpiperazine | HCID 78013 | — |
| Reactant | 8-chlorodibenz[b,f][1,4]oxazepin-10(11H)carbonyl chloride | HCID 14975983 | — |
| Product | HCID 15224910 | HCID 15224910 | 89.2% |
Reaction Steps
The title compound of Example 2 (1.0 g, 3.4 mmol) was combined with 1-(1-methylethyl)piperazine (0.48 g, 3.7 mmol) and the reaction was carried out by the method of Example 4. Following chromatographic purification, 1.17 g of the title product was obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05354747 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-4a1b26e021be4bdd8b8aecf9068972fb |
| Source note | uspto-grants-1994_10 |