HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazine → 1-[2-(4-Pyridinyl)ethyl]piperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazine | HCID 4837 | — |
| Reactant | 4-Vinylpyridine | HCID 7502 | — |
| Product | 1-[2-(4-Pyridinyl)ethyl]piperazine | HCID 558685 | 40.1% |
Reaction Steps
To a melt of piperazine (15 g, 0.17 mol) heated to 105° C. was added dropwise 4-vinylpyridine (1.25 mL, 0.012 mol). After refluxing the reaction for 5.5 hours, it was cooled to room temperature and chromatographed to provide 0.92 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05354747 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-d993ab5620a446f4b33f5a57a94925a0 |
| Source note | uspto-grants-1994_10 |