1-Methoxy-4-nitro-3-(2-nitroethenyl)-2-(phenylmethoxy)benzene → HCID 18962537, compound
Reaction equation
[CH2:1]([O:8][C:9]1[C:19]([O:20][CH2:21]C)=[CH:18][CH:17]=[C:16]([N+:23]([O-])=O)[C:10]=1[CH:11]=[CH:12][N+]([O-])=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(OC1C(OC)=CC=C([N+]([O-])=O)C=1C=C[N+]([O-])=O)C1C=CC=CC=1>>[CH2:1]([O:8][C:9]1[C:19]([O:20][CH3:21])=[CH:18][CH:17]=[C:16]2[C:10]=1[CH:11]=[CH:12][NH:23]2)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1Participants
3
Procedure
This compound is obtained according to the operating method described in Example lc, in which the 2-benzyloxy-3-ethoxy-6,β-dinitrostyrene is replaced with 2-benzyloxy-3-methoxy-6,β-dinitrostyrene. A white powder (yield =86%, m.p. =83°-84° C.) is obtained.
Workup
- customThis compound is obtained
- customA white powder (yield =86%, m.p. =83°-84° C.)
- customis obtained
Sources & evidence
- ORD record
- ord-c2e58fcda7624d2cbc2e2cad00bfeb96
- Source dataset
- uspto-grants-1994_10
- Patent number
- US05354870
Reaction notes
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