HCID 57070113, compound → HCID 18962534, compound
Reaction equation
[CH2:1]([O:8][C:9]1[C:20]([O:21][CH2:22]C)=[CH:19][CH:18]=[C:17](C[N+]([O-])=O)[C:10]=1[CH:11]=[CH:12][CH2:13][N+]([O-])=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(OC1C(OC)=CC=C(C[N+]([O-])=O)C=1C=CC[N+:41]([O-])=O)C1C=CC=CC=1>>[CH2:1]([O:8][C:9]1[C:20]([O:21][CH3:22])=[CH:19][CH:18]=[C:17]2[C:10]=1[CH:11]=[C:12]([CH3:13])[NH:41]2)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1Participants
3
Procedure
This compound is obtained according to the operating method described in Example 2b, in which the 2-benzyloxy-3-ethoxy-6,β-dinitromethylstyrene is replaced with 2-benzyloxy-3-methoxy-6,β-dinitromethylstyrene. A pale yellow powder (yield =40%, m.p. =74°-75° C.) is obtained.
Workup
- customThis compound is obtained
- customA pale yellow powder (yield =40%, m.p. =74°-75° C.)
- customis obtained
Sources & evidence
- ORD record
- ord-7e71375090f74783b10d64e1e2ac93a2
- Source dataset
- uspto-grants-1994_10
- Patent number
- US05354870
Reaction notes
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