Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Quinoline | HCID 7047 | — |
| Reactant | HCID 18962694 | HCID 18962694 | — |
| Catalyst | Lindlars catalyst | HCID 131709914 | — |
| Product | HCID 18962696 | HCID 18962696 | 90% |
Reaction Steps
100 g of 3,4,4-trimethylhex-1-yn-3-ol, 3 g of quinoline and 5.4 g of Lindlar catalyst were initially introduced in 100 ml of petroleum ether and the mixture was stirred at 25° C. for 10 hours under a hydrogen atmosphere. The catalyst was then filtered off, the filtrate was concentrated and the residue was analyzed by means of GC. 91 g (90%) of 3,4,4-trimethylhex-1-en-3-ol were obtained. The residue was processed without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05354937 |
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| Source dataset | uspto-grants-1994_10 |
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| ORD ID | ord-d0ef38c552cc49dca9e163e77182db3b |
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| Source note | uspto-grants-1994_10 |
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