Phosphoric Acid → HCID 18962695, compound

Participants

Reaction Steps

40 g of 3,4,4-trimethylhex-1-en-3-ol were added dropwise to a mixture of 200 g of polyethylene glycol and 3 g of phosphoric acid at from 285° C. to 290° C. in the course of 2 hours. The organic phase of the two-phase mixture discharged was analyzed by means of GC. 24 g (70%) of 2-tert-amylbutadiene were obtained. The organic phase was processed without purification.

Provenance & Evidence