Procysteine → HCID 44285036, compound

HRID 1708192Notes

Reaction equation

HRID 1708192 reaction equation
[O:1]=[C:2]1[NH:6][C@H:5]([C:7]([OH:9])=O)[CH2:4][S:3]1.[N+]([O-])(O)=O.[N+:14]([O:17][CH:18]([CH3:21])[CH2:19][NH2:20])([O-:16])=[O:15]>>[N+:14]([O:17][CH:18]([CH3:21])[CH2:19][NH:20][C:7]([C@@H:5]1[CH2:4][S:3][C:2](=[O:1])[NH:6]1)=[O:9])([O-:16])=[O:15]

Participants

3

Reactant 2

HCID 72390ProcysteineHCID 86747701HCID 86747701, compound

Product 1

HCID 44285036HCID 44285036, compound

Procedure

A procedure similar to that described in Example 1 was repeated, but using 2.0 g of (4R)-2-oxothiazolidine4-carboxylic acid and 3.0 g of N-(2-nitrooxypropyl)amine nitrate, to obtain 24 mg of the title compound as pale yellow crystals, melting at 70°-72° C. (after recrystallization from ethanol).

Workup

  1. customto obtain
  2. custom24 mg of the title compound as pale yellow crystals, melting at 70°-72° C. (after recrystallization from ethanol)

Sources & evidence

ORD record
ord-a8685ec43095407a8f44a0938fe6e686
Source dataset
uspto-grants-1994_10
Patent number
US05356918

Reaction notes

Loading…