HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) → N-(2-Nitrooxyethyl)-2-oxo-5-(2-thienyl)oxazolidine-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) | HCID 78397 | — |
| Reactant | 2-Oxo-5-(2-thienyl)oxazolidine-4-carboxylic acid | HCID 18961045 | — |
| Product | N-(2-Nitrooxyethyl)-2-oxo-5-(2-thienyl)oxazolidine-4-carboxamide | HCID 18961051 | 26.9% |
Reaction Steps
A procedure similar to that described in Example 19 was repeated, but using 500 mg of 2-oxo-5-(2-thienyl)oxazolidine-4-carboxylic acid and 480 mg of N-(2-nitrooxyethyl)amine nitrate, to obtain 190 mg of the title compound as pale yellow plates, melting at 101°-103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05356918 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-e4c03a36f0a64ed99b3fbce5b661f941 |
| Source note | uspto-grants-1994_10 |