HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trimethylpyridine → HCID 44285578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trimethylpyridine | HCID 7953 | — |
| Reactant | Nitronium tetrafluoroborate | HCID 11073463 | — |
| Reactant | HCID 54320074 | HCID 54320074 | — |
| Product | HCID 44285578 | HCID 44285578 | 20.9% |
Reaction Steps
Following a procedure similar to that described in Example 16(b), but using 195 mg of nitronium tetrafluoroborate, 157 mg of 2,4,6-collidine and 218 mg of (4R)-N-(4-hydroxybutyl)-2-oxothiazolidine-4-carboxamide [prepared as described in step (a) above], 55 mg of the title compound were obtained as colorless needles, melting at 68°-70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05356918 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-c53d8d2b5f154a1cb76e87ad5d77b17b |
| Source note | uspto-grants-1994_10 |