HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53659360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19030984 | HCID 19030984 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 53659360 | HCID 53659360 | — |
Reaction Steps
To a solution of 1-(4-carboxyphenyl)-3,4-dihydrocarbostyril (0.2 g) in chloroform (5 ml) is added thionyl chloride (0.8 ml) and the mixture is refluxed with h eating for 1 hour. Then, chloroform and thionyl chloride are distilled off under reduced pressure to give 4-(3,4-dihydrocarbostyril-1-yl)benzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05356904 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-74dd2312ca914befb6f1583ce1ad17c1 |
| Source note | uspto-grants-1994_10 |