Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 2724782 | HCID 2724782 | — |
Reaction Steps
To 758 g (7.7 moles) of cyclohexanone were added 260 g (1.44 moles) of anhydrous dextrose, followed by 20 ml of concentrated sulfuric acid. The mixture was heated to 35° C. and monitored by TLC. The flow rate of the desired product using Solvent A was Rf =0.95.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05358936 |
|---|
| Source dataset | uspto-grants-1994_10 |
|---|
| ORD ID | ord-cc1b381f737544b69d632a33c4abc61f |
|---|
| Source note | uspto-grants-1994_10 |
|---|
