HCID 1731445, compound → HCID 1204317, compound

Participants

Reaction Steps

A solution of N-(3-nitrophenyl)-4-nitro phthalimide (5.0 g. ) in tetrahydrofuran (300 ml) was reduced under hydrogen (45 psi) using platinum oxide catalyst (0.2 g.) for 18 hours. The solution was dried (MgSO4), filtered through Celite, and the solvent evaporated under reduced pressure to yield 4-amino-N-(3-aminophenyl)phthalimide; 3.8 g. (93.1%); M.P. 228-231°. Calcd. for C14H11N3O2 : C, 66.4; H, 4.4; N, 16.6. Found: C, 66.9; H, 4.9; N, 16.0.

Provenance & Evidence