Diethyl Ether → HCID 14461248, compound

Participants

Reaction Steps

1.8 g (5.5 mmol) of the compound from Example 7a in 30 ml of dichloromethane are poured into a suspension of 1.8 g (0.4 mmol) of PCC in 30 ml of dichloromethane at room temperature. After stirring at room temperature for 3 h, 3 volumes of ether are added, and the mixture is filtered through silica gel. Removal of the solvent in vacuo, and chromatography on silica gel (cyclohexane/ethyl acetate 1) yields 1.5 g of the title compound as a solid.

Provenance & Evidence