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HRID1708882

反应详情

EQUATION

反应方程式

HRID 1708882 的结构方程式

REACTANTS

反应物

3
结构：c1ccncc1
HCID1049

Pyridine

C5H5N

结构：CSC(=NC#N)SC
HCID66289

Dimethyl cyanocarbonodithioimidate

C4H6N2S2

结构：C[C@@H]1CC(=O)NN=C1c1ccc(N)cc1
HCID10465484

(5R)-6-(4-Aminophenyl)-4,5-dihydro-5-methyl-3(2H)-pyridazinone

C11H13N3O

PRODUCTS

生成物

1
结构：CSC(=N)N(C#N)c1ccc(C2=NNC(=O)C[C@H]2C)cc1
HCID131716492

未命名化合物

PROCEDURE

实验过程

A stirred mixture of (R)-6-(4-aminophenyl)-5-methyl-4,5-dihydro-3(2H)-pyridazinone (4 g) and dimethyl cyanodithioiminocarbonate in pyridine is heated to afford (R)-6-(4-(N-cyano-S-methylisothioureido)phenyl)-5-methyl-4,5-dihydro-3(2H)-pyridazinone.

WORKUP

后处理

  1. temperatureis heated