HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 14774344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Chloro-4,5-dipropargyloxybenzoic acid | HCID 14130319 | — |
| Product | HCID 14774344 | HCID 14774344 | — |
Reaction Steps
A mixture of 3-chloro-4,5-dipropargyloxybenzoic acid (10.7 g) and thionyl chloride (30 ml) was stirred under reflux for 1 hour. After cooling, the reaction mixture was evaporated under reduced pressure to give 3-chloro-4,5-dipropargyloxybenzoyl chloride in a quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04946865 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-07ff82ca74c44a7dbdba0967f16cd488 |
| Source note | uspto-grants-1990_08 |