Hydrochloric Acid → HCID 23039021, compound

Participants

Reaction Steps

12 g of N,N-dipropyl-1-hydroxy-6-methoxy-1-indanmethylamine were dissolved in 100 milliliters of methanol and 7 milliliters of concentrated hydrochloric acid and reduced catalytically with hydrogen at 3 atmospheres and 50 degrees Centigrade for 20 hours with 10 g of 5% palladium on carbon black containing 50% of water as a catalyst. After filtration of the catalyst and evaporation of the methanol 13 grams of product were obtained. The oxalate was precipitated from acetone. M.P. 124°-130° C.

Provenance & Evidence