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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1708987Generated: October 31, 2026

HCID 73553870, compound → HCID 58051386, compound

https://huagongshe.com/reaction/1708987

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 73553870HCID 73553870—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 58051386HCID 5805138683.2%

Reaction Steps

50 g of 5-methoxy-3-benzofuranacetic acid methylester were dissolved in 200 ml of ethanol, and 18 g of 5% Pd on carbon black (50% water) were added. Hydrogenation was performed at 3 ato. for 4 hours at 65° C. The catalyst was filtered off, and ethanol evaporated yielding 42 g of an oil, which was not further purified before use in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04946863
Source datasetuspto-grants-1990_08
ORD IDord-9ffea6df0c8d4ad780f82d12b1726fd5
Source noteuspto-grants-1990_08