Dibenzoylmethane → HCID 14573625, compound

HRID 1709012Notes

Reaction equation

[C:1]1([C:7](=[O:17])[CH2:8][C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:18]([NH:20][C:21](=[O:24])[CH:22]=[CH2:23])O>>[C:11]1([C:9](=[O:10])[CH:8]([CH2:18][NH:20][C:21](=[O:24])[CH:22]=[CH2:23])[C:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)=[O:17])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

Reactant 2

HCID 8433Dibenzoylmethane

HCID 13543N-Methylolacrylamide

Product 1

HCID 14573625HCID 14573625, compound

Procedure

1,3-Diphenyl-2-(acrylamidomethyl)-propane-1,3-dione was prepared from 143 g of 1,3-diphenylpropane-1,3-dione and 64.8 g of N-methylolacrylamide similarly to the method described in Synthesis Example I.

Workup

customdescribed in Synthesis Example I

Sources & evidence

ORD record: ord-4cd5720b8fff4b1b97a8cf0705159500
Source dataset: uspto-grants-1990_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04946917

Reaction notes

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