HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1709020Generated: October 31, 2026
HCID 23039154, compound → HCID 86744136, compound
https://huagongshe.com/reaction/1709020
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 23039154 | HCID 23039154 | — |
| Solvent | Styrene | HCID 7501 | — |
| Product | HCID 86744136 | HCID 86744136 | 96.2% |
Reaction Steps
A solution of 1.00 percent by weight m-(t-butylazo)-styrene in styrene monomer is heated for 14 hours at 130° C. in a vacuum ampoule. Thereafter, the ampoule is opened and heated for 1 hour at 210° C. and 10 mm Hg pressure to remove unreacted monomer. An m-(t-butylazo)-styrene/styrene copolymer is obtained in a 96.2 percent yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04946949 |
|---|
| Source dataset | uspto-grants-1990_08 |
|---|
| ORD ID | ord-4daee5cbb2c1404d8b61e0d2967c62a5 |
|---|
| Source note | uspto-grants-1990_08 |
|---|