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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1709020Generated: October 31, 2026

HCID 23039154, compound → HCID 86744136, compound

https://huagongshe.com/reaction/1709020

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 23039154HCID 23039154—
SolventStyreneHCID 7501—
ProductHCID 86744136HCID 8674413696.2%

Reaction Conditions

Temperature210 °C

Reaction Steps

A solution of 1.00 percent by weight m-(t-butylazo)-styrene in styrene monomer is heated for 14 hours at 130° C. in a vacuum ampoule. Thereafter, the ampoule is opened and heated for 1 hour at 210° C. and 10 mm Hg pressure to remove unreacted monomer. An m-(t-butylazo)-styrene/styrene copolymer is obtained in a 96.2 percent yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04946949
Source datasetuspto-grants-1990_08
ORD IDord-4daee5cbb2c1404d8b61e0d2967c62a5
Source noteuspto-grants-1990_08