HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(tert-butoxycarbonyl)glycine → HCID 18640552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(tert-butoxycarbonyl)glycine | HCID 78288 | — |
| Reactant | 2,4,6-Tris(1-methylethyl)benzenesulfonyl chloride | HCID 81042 | — |
| Reactant | HCID 10806767 | HCID 10806767 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18640552 | HCID 18640552 | — |
Reaction Steps
To a solution of 1.00 g of 5'-O-benzyl-2'-deoxy-5-fluorouridine in 30 ml of anhydrous pyridine were added 0.78 g of N-(t-butoxycarbonyl)glycine and 1.80 g of 2,4,6-triisopropylbenzenesulfonyl chloride, and the mixture was subjected to reaction at room temperature overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04946951 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-ae2148677245431d9b7426750fe4a539 |
| Source note | uspto-grants-1990_08 |