4-Pentylbenzoic acid → HCID 178444557, compound

HRID 1709153Notes

Reaction equation

HRID 1709153 reaction equation
[CH2:1]([C:6]1[CH:14]=[CH:13][C:9]([C:10]([OH:12])=[O:11])=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5].C([C@H]1CC[C@H](C(O)=O)CC1)CCC>>[CH2:1]([C@H:6]1[CH2:7][CH2:8][C@H:9]([C:10]([OH:12])=[O:11])[CH2:13][CH2:14]1)[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

3

Reactant 2

HCID 334794-Pentylbenzoic acidHCID 178445662HCID 178445662, compound

Product 1

HCID 178444557HCID 178444557, compoundYield 80%

Procedure

This compound was prepared from 4-n-pentylbenzoic acid (15, 53.8 g, 0.28 mol), in a manner similar to the procedure described for trans-4-n-butylcyclohexanecarboxylic acid (11) in Example I, Preparation 1 in an overall yield of 80% (43 g); m.p. 50-51° C. (pet. ether).

Sources & evidence

ORD record
ord-1d0843aefa2e447891ba2ed57fec3f04
Source dataset
uspto-grants-1990_08
Patent number
US04948790

Reaction notes

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