Benzoic acid, 4-hexyl- → HCID 178443910, compound

HRID 1709154Notes

Reaction equation

HRID 1709154 reaction equation
[CH2:1]([C:7]1[CH:15]=[CH:14][C:10]([C:11]([OH:13])=[O:12])=[CH:9][CH:8]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].C([C@H]1CC[C@H](C(O)=O)CC1)CCC>>[CH2:1]([C@H:7]1[CH2:8][CH2:9][C@H:10]([C:11]([OH:13])=[O:12])[CH2:14][CH2:15]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Participants

3

Reactant 2

HCID 30725Benzoic acid, 4-hexyl-HCID 178445662HCID 178445662, compound

Product 1

HCID 178443910HCID 178443910, compoundYield 60%

Procedure

This compound was prepared from 4n-hexylbenzoic acid (18, 72.34 g, 0.28 mol), in a manner similar to the procedure described for trans-4-n-butylcyclohexanecarboxylic acid (11) in Example I, Preparation 1, in an overall yield of 60% (35.7 g), m.p. 30+C. (pet. ether).

Sources & evidence

ORD record
ord-2cfa76ae9ffa4cc199096f7320a3c4d6
Source dataset
uspto-grants-1990_08
Patent number
US04948790

Reaction notes

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