Isoamyl Alcohol → HCID 15696560, compound

HRID 1709191Notes

Reaction equation

HRID 1709191 reaction equation
[CH2:1]([O:3][CH:4]1[NH:8][C:7](=[O:9])[CH2:6][CH2:5]1)[CH3:2].[CH3:10][CH:11](C)[CH2:12]CO>>[CH3:10][CH:11]([CH3:12])[CH2:2][CH2:1][O:3][CH:4]1[NH:8][C:7](=[O:9])[CH2:6][CH2:5]1

Participants

3

Reactant 2

HCID 31260Isoamyl AlcoholHCID 35805555-Ethoxy-2-pyrrolidinone

Product 1

HCID 15696560HCID 15696560, compound

Procedure

5.5 g of 5-ethoxy-pyrrolidin-2-one, 30 cm3 of 3-methyl-butanol and 2.75 g of Amberlite-15 resin are agitated for 5 hours at ambient temperature. After leaving in the refrigerator for 18 hours, there is obtained, after filtering, 4.1 g of the expected product. m.p. 73°-75° C.

Workup

  1. customAfter leaving in the refrigerator for 18 hours
  2. customthere is obtained
  3. filtrationafter filtering

Sources & evidence

ORD record
ord-7e61fa161c2e44459615fd1be72a85ff
Source dataset
uspto-grants-1990_08
Patent number
US04948804

Reaction notes

Loading…