HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11074035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11020199 | HCID 11020199 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11074035 | HCID 11074035 | — |
Reaction Steps
A solution of 0.5 g (2.4 mmol) N-methyl-4,5-dimethoxy-2-nitroanilin in 150 ml ethanol was added 1 ml 4N hydrochloric acid, and the mixture was hydrogenated at atm. pressure by using 5% Pd-C (0,1 g) as a catalyst. The reaction mixture was filtered and evaporated in vacuo to give 2-amino-4,5-dimethoxy-N-methylaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04948794 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-1bdcaf3585c4493883d47fafb6eebc34 |
| Source note | uspto-grants-1990_08 |