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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1709352Generated: October 30, 2026

Cyanuric chloride → 2-[N,N-bis(2,2,6,6-tetramethyl-4-piperidyl)amino]-4,6-dichloro-1,3,5-triazine

https://huagongshe.com/reaction/1709352

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyanuric chlorideHCID 7954—
ReactantSodium HydroxideHCID 14798—
Reactant2,2,6,6-Tetramethyl-N-(2,2,6,6-tetramethyl-4-piperidinyl)-4-piperidinamineHCID 566708—
SolventO-XyleneHCID 7237—
Product2-[N,N-bis(2,2,6,6-tetramethyl-4-piperidyl)amino]-4,6-dichloro-1,3,5-triazineHCID 14365120—

Reaction Conditions

Temperature0 °C

Reaction Steps

29.5 g (0.1 mol) of bis(2,2,6,6-tetramethyl-4-piperidyl)amine are slowly added to a solution, cooled to -10° C., of 18.45 g (0.1 mol) of cyanuric chloride in 160 ml of xylene, maintaining the temperature at about 0° C. After the end of the addition, the mixture is stirred for 3 hours at room temperature, 4.4 g (0.11 mol) of powdered sodium hydroxide are added and stirring is continued for a further 2 hours at room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04948889
Source datasetuspto-grants-1990_08
ORD IDord-5bd5713005f94787b5cda20ba0c8664d
Source noteuspto-grants-1990_08