HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-(3,4-Dichlorobenzyl)-5-methylamino-1,2,3-triazole-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-Amino-1-(3,4-dichlorobenzyl)-1,2,3-triazole-4-carboxamide | HCID 14033033 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-(3,4-Dichlorobenzyl)-5-methylamino-1,2,3-triazole-4-carboxamide | HCID 23036237 | — |
Reaction Steps
A mixture of 5-amino-1-(3,4-dichlorobenzyl)-1,2,3-triazole-4-carboxamide (2.86 g, 10.0 mmol), methyl iodide (1.42 g, 10.0 mmol), and potassium carbonate (1.38 g, 10.0 mmol) in N,N-dimethylformamide (20 ml) is stirred 48 hours a ambient temperature, poured into water (150 ml), and filtered. Chromatography provides 1-(3,4-dichlorobenzyl)-5-methylamino-1,2,3-triazole-4-carboxamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04950673 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-6837611dea994989bd22b55aa5b1be0b |
| Source note | uspto-grants-1990_08 |