HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 23036214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 23036239 | HCID 23036239 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23036214 | HCID 23036214 | 89% |
Reaction Steps
A solution of 4-methyl-3-(trichlorovinyl)benzyl chloride (1.81 g ) and sodium azide (650 mg) in 20 ml of ethanol was heated at reflux for 5 hours. The reaction mixture was concentrated and then chromatographed on silica gel. Elution with 1:1 hexane:methylene chloride afforded 1.65 g of pure azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04950673 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-6593f2e0dab2459b8c08ec9b98ffa7aa |
| Source note | uspto-grants-1990_08 |