HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → Ethyl 5-ethoxy-2-hydroxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Ethyl 2,5-dihydroxybenzoate | HCID 77548 | — |
| Product | Ethyl 5-ethoxy-2-hydroxybenzoate | HCID 4419976 | 69.8% |
Reaction Steps
Using the general method of Example XXIII Part A, 31.2 g (0.20 mole) of ethyl iodide was reacted with 27.3 g (0.15 mole) of ethyl 2,5-dihydroxybenzoate to provide 22 g of white crystalline ethyl 5-ethoxy-2-hydroxybenzoate, m.p. 64°-66° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04952574 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-f273db21349e4f038a6a1812f2c00c42 |
| Source note | uspto-grants-1990_08 |