Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | Propylamine | HCID 7852 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11310181 | HCID 11310181 | 97,590.398% |
Reaction Steps
A mixture of 118.6 g (1.67 mol) of acrylamide and 49.3 g (0.83 mmol) of 1-aminopropane in 250 ml of methanol was heated at 80° C. for 1 hour. The solvent was evaporated and the solid crystallized from ethanol. There was obtained 162.3 g (0.81 mol, 97%) of 3,3'-(propylimino)bispropanamide as a white solid mp 101°-101.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04952583 |
|---|
| Source dataset | uspto-grants-1990_08 |
|---|
| ORD ID | ord-f70d2ae5049e4d698e0d8bf08cd97012 |
|---|
| Source note | uspto-grants-1990_08 |
|---|
