HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 110003-21-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3,4,4-Trifluoro-3-butene-1-amine | HCID 15239145 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 110003-21-9 | HCID 15239144 | — |
Reaction Steps
A stirred solution of 0.4 gram (0.004 mole) of 4-amino-1,1,2-trifluoro-1-butene in 25 ml of diethyl ether was saturated with gaseous hydrochloric acid. The reaction mixture was concentrated under reduced pressure to give 0.4 gram of 4-amino-1,1,2-trifluoro-1-butene hydrochloride as a solid. The nmr spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04952580 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-703994b28af04b21b0f3112fbf7b8bc6 |
| Source note | uspto-grants-1990_08 |