HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenanthro[1,2-b]furan-2-carbaldehyde → Phenanthro[1,2-b]thiophene-2-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenanthro[1,2-b]furan-2-carbaldehyde | HCID 14770240 | — |
| Reactant | Phenanthro[1,2-b]thiophene-2-methanol | HCID 14770248 | — |
| Solvent | Methylenechloride Hexane | HCID 21226440 | — |
| Product | Phenanthro[1,2-b]thiophene-2-carbaldehyde | HCID 14770249 | 82.9% |
Reaction Steps
Using the procedure outlined in 14B, phenanthro[1,2-b]thiophene-2-methanol (16A) gave a 82.9% yield of phenanthro[1,2-b]thiophene-2-carbaldehyde, mp 209°-210°, (C,H,S), (CH2Cl2 /hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04952597 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-aadc558436174dcab40ec2c1140e2088 |
| Source note | uspto-grants-1990_08 |