HCID 15077157, compound → HCID 15077158, compound

HRID 1710165Notes

Reaction equation

HRID 1710165 reaction equation
[O:1]1[C:5]([CH2:6][OH:7])=[CH:4][C:3]2[CH:8]=[CH:9][C:10]3[CH:11]=[CH:12][C:13]4[CH:14]=[CH:15][CH:16]=[CH:17][C:18]=4[C:19]=3[C:2]1=2>CCO.C(Cl)Cl>[O:1]1[C:5]([CH:6]=[O:7])=[CH:4][C:3]2[CH:8]=[CH:9][C:10]3[CH:11]=[CH:12][C:13]4[CH:14]=[CH:15][CH:16]=[CH:17][C:18]=4[C:19]=3[C:2]1=2

Participants

3

Reactant 1

HCID 15077157HCID 15077157, compound

Product 1

HCID 15077158HCID 15077158, compoundYield 91.2%

Reagents, catalysts & solvents 1

HCID 21584144Dichloromethane ethanolSolvent

Procedure

Using the procedure outlined in Example 14B, phenanthro[4,3-b]furan-2-methanol (18A) gave a 91.2% yield of phenanthro[4,3-b]furan-2-carbaldehyde, mp 169°, (C,H), (95% EtOH/CH2Cl2).

Sources & evidence

ORD record
ord-8a6dc023f274489199091e41b594a12c
Source dataset
uspto-grants-1990_08
Patent number
US04952597

Reaction notes

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