HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitroethane → HCID 13358884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | 1-Hexene | HCID 11597 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13358884 | HCID 13358884 | — |
Reaction Steps
A reactor was charged with 20.0 parts phthalic anhydride, 20.9 parts nitroethane, 34.0 parts 1-hexene and heated to reflux. Then, 13.8 parts of triethylamine was slowly added over a one hour period. The mixture was refluxed for 20 hours. The product mixture was vacuum fractionally distilled to provide 3-methyl-5-butylisoxazoline in good yields.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04952700 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-a4177058d19c411bb60e4bc1cfbc9aca |
| Source note | uspto-grants-1990_08 |