Triethylamine → HCID 14418810, compound

Participants

Reaction Steps

4-(2-n-Nonyl-1,3,4-thiadiazole-5-yl)-benzoic acid (0.005 moles, 1.66 g) is reacted with 5 mL of thionyl chloride and heated 2 hours at the boiling point. After that, the excess thionyl chloride is distilled off in the rotary evaporator and the residue is treated with 0.006 moles (1.33 g) octyloxyphenol, dissolved in 20 mL toluene, 5 mL triethylamine and 100 mg 4-dimethylaminopyridine.

Provenance & Evidence