HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 1-Methyl-1H-pyrrolo[2,3-b]pyridine-3-carboxaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,3-Dimethylindole | HCID 70130 | — |
| Reactant | N-methyl-7-azaindole | HCID 583068 | — |
| Product | 1-Methyl-1H-pyrrolo[2,3-b]pyridine-3-carboxaldehyde | HCID 10441960 | 47% |
Reaction Steps
According to the procedure of Preparation 40 (b), except substituting 1-methyl-1H-pyrrolo[2,3-b]pyridine (0.7 g, 5.3 mmole) for the 1,3-dimethylindole, the title compound (0.4 g, 47%) was prepared as a white solid: MS (ES) m/e 161 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790716B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-eff1f842384b42a7a4af65ad4b44c6d1 |
| Source note | uspto-grants-2010_09 |