HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → (Pyridin-2-ylsulfanyl)-acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 2-pyridin-2-ylsulfanylacetate | HCID 15388132 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (Pyridin-2-ylsulfanyl)-acetic acid | HCID 654661 | 95% |
Reaction Steps
A solution of the ester from above (751 mg, 4.10 mmol) in MeOH (50 ml) and 1N NaOH (10 ml) was stirred at room temperature for 45 minutes to give (pyridin-2-ylsulfanyl)-acetic acid (655 mg, 95%) after acidic work-up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790747B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-2253ce553bff44268f3d42805d563042 |
| Source note | uspto-grants-2010_09 |